Whether for energy applications or nuclear waste management, industrial processing of aluminum requires understanding its behavior in highly alkaline solutions. Processing slurries and precipitates (typically gibbsite, α-Al(OH)3) from these solutions is aided by controlling the shape of tiny particles that are produced. Researchers at the IDREAM Energy Frontier Research Center, funded by DOE’s Office of Science, Basic Energy Sciences, developed a synthesis route. The scientists devised the route based on simple, rational design principles. With it, the team produced highly uniform gibbsite nanoplates with optimal yield.